Analysis of substituted amides present in primary amines

Chromatography Forum: GC Archives: Analysis of substituted amides present in primary amines
Top of pagePrevious messageNext messageBottom of pageLink to this message  By YLB on Wednesday, March 5, 2003 - 08:39 am:

HELP!!!! I am trying to detect substituted amides present in a primary amide. This is a C36 amide, and the response is LOW. I am using GC with a capillary column, and I am having no luck...what can I do?


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Wednesday, March 5, 2003 - 05:55 pm:

You need to be more specific... C36 amide on FID should respond well on any non-polar column. Use a short column, fast flow, high starting temp as a start.


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