By Anonymous on Thursday, June 19, 2003 - 05:32 am:
I currently have a DB5 equivalent capillary column
(30m x 0.25mm id x 0.25um) and I want to try a 0.10mm id column for "faster" chromatography.
Can anyone suggest a suitable starting point - in terms of dimensions and ramp rates etc?
I run at 1ml/min Helium 70 - 300degC at 4degC/min.
My injector is suitable and I use a FID.
Injection 0.1 - 0.2uL at 200:1.
(Hydrogen as a carrier is not an option!)
Has anyone had experiences / problems in translating methods across?
By Ralph on Thursday, June 19, 2003 - 08:44 am:
Agilent have a good free program:
http://www.chem.agilent.com/cag/servsup/usersoft/main.html#mxlator
Regards,
Ralph