Hydrogen detection

Chromatography Forum: GC Archives: Hydrogen detection
Top of pagePrevious messageNext messageBottom of pageLink to this message  By shyam s Reddy on Wednesday, August 25, 2004 - 11:45 pm:

I am trying to calibrate the GC with pure hydrogen. I am getting a sharp and tall peak for h2 within 1 minute of injection in TCD mode.Oven temp 80deg,injection port temp 60deg, column is mol sieve 5A,carrier gas nitrogen 30ml/min.All these parameters are ok or not.What should be the temparature of the detector. Please suggest me any good parameters.
Thanking you,
gss reddy

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