Sample Prep

Chromatography Forum: LC Archives: Sample Prep
Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Monday, June 14, 1999 - 10:10 am:

From time to time we find ourselves needing to prep from a "jelly" sample matrix. We can extract out part of the matrix, but find the initial "jelly" hard to quantify.


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Steve B on Tuesday, June 15, 1999 - 08:09 am:

Is this a carbohydrate, protein, or synthetic jelly?


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Tuesday, June 15, 1999 - 08:57 am:

We do not deal with biological samples, this is a synthetic "jelly"


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Dennis Saunders on Friday, July 2, 1999 - 05:41 pm:

I have handled petroleum jelly samples by dissolving is hot hexane or heptane. I then extract the hexane solution solution with methanol.

Synthetic polymers like SBRs and acrylics are often crosslinked. Attempting to dissolve them causes the cross-linked network to swell into a gel. Quantitative extractions of the soluble material can be accomplished only with long extraction times.


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