3-Chloroperbenzoic Acid [937-14-4]

Chromatography Forum: LC Archives: 3-Chloroperbenzoic Acid [937-14-4]
Top of pagePrevious messageNext messageBottom of pageLink to this message  By Carlos Teixeira on Monday, March 25, 2002 - 06:29 am:

Hi My Friends;

I need of the Method to analyse the
Assay of 3-Chloroperbenzoic Acid
[937-14-4].

Help me please.


Carlos Teixeira
teixeiracs@yahoo.com


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Monday, March 25, 2002 - 08:05 am:

Wet chemistry offers the best solution (pardon the pun).
How does one measure the oxidizing potential of a strong peroxide? Any wet chemistry wizards out there have an answer.
The raw material often contains several percent of the reduced free acid. Once completedly reduced a methyl ester derivative run on a polar GC column will give you the isomer purity; but that is not your question or your problem, I would guess.


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Carlos Teixeira on Monday, March 25, 2002 - 11:11 am:

Hi Anonymous,

Tank for your help. I will try to derivate my sample.

Carlos Teixeira
teixeiracs@yahoo.com


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