I would like to analyse lincomycin in feed by HPLC and I would like to know if there is someone that is working in this field. I need some help to start and if there was some bibliographic reference to start it, I would be very grateful.
Ana Guillén
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By Mel on Wednesday, October 23, 2002 - 08:31 am:
Determination of clindamycin in animal plasma by high-performance liquid chromatography combined with electrospray ionization mass spectrometry.
J Mass Spectrom. 2002 Aug;37(8):848-53.
This reference used lincomycin as an internal standard.
As a starting point for all of my literature searches I use medline which can be found at:
http://www.ncbi.nlm.nih.gov/entrez/query.fcgi
Mel
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By Anonymous on Wednesday, October 23, 2002 - 11:45 am:
Here are some more references:
1. Identification and determination of oxytetracycline, tiamulin, lincomycin, and spectimycin in veterinary preparations by thin-layer chromatography-densitometry
J. Assoc. Off. Anal. Chem. 83 (2000) 1502-1506 Krzek, J., Kwiecien, A., Starek, M., Kierszniewska, A. and Rzeszutko, W.
Technique: PC;
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2. Liquid chromatographic method for separation of lincomycin from its related substances
J. Chromatogr. A 829 (1998) 161-166 Orwa, J.A., Bosmans, F., Depuydt, S., Roets, E. and Hoogmartens, J.
Technique: LC;
[Full text supplied by Science Direct] [Free abstract]
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3. High performance liquid chromatographic determination of lincomycin in pharmaceutical formulations
J. Serb. Chem. Soc. 62 (1997) 1221-1225 Vladimirov, S., Markovic, L., Agbaba, D., Zivanov-Stakic, D. and Brboric, J. C.A., 128 (1998) 53345j.
Technique: LC;
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8. Determination of lincomycin in milk and tissues by reversed-phase liquid chromatography.
J. Agric. Food Chem. 39 (1991) 1812-1816 Moats, W.A.
Technique: LC;
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9. Development of an efficient HPLC analysis for lincomycin for use in contract laboratories.
Methodol. Surv. Biochem. Anal. 20 (Anal. Drugs Metab., Incl. Anti-Infect. Agents) (1990) 117-122 James, C.A., Simmonds, R.J. and Wood, S.A. C.A., 114 (1991) 62u.
Technique: LC;
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Hope this helps.
Melissa