Carboxylate anoins determination

Chromatography Forum: LC Archives: Carboxylate anoins determination
Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Tuesday, April 1, 2003 - 03:38 am:

Hi,
I wish to determine total content of Carboxylate anions in castor oil ?? Please advice what sort of method should i try??

thanks


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Tuesday, April 1, 2003 - 02:56 pm:

In the spirit of the day, I suggest to eat the castor oil and measure the pH as it comes out again. Compare the pH to a reference standard!


Top of pagePrevious messageNext messageBottom of pageLink to this message  By bill tindall on Tuesday, April 1, 2003 - 04:45 pm:

titration


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Tuesday, April 1, 2003 - 11:55 pm:

since the total free anions would be very low in sample , i do not see titration/pH will help in such a situation??


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Thursday, April 3, 2003 - 03:56 am:

Do you mean Free Fatty Acids in vegable oil ???
For total FFA use titration.
If you need to characterise the different FFA, and you want only to report up to C5-C6 chain long then it can be done by IC
Though the best way will probably be GC


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