for some weeks now I ame faced with a problem with two Waters 996 PDA-detector in our lab. The baseline of these PDA's is going up and down in about 8 min. these symtomps are there pumping elluens and without pumping elluens. When I monitored the baseline of the two PDA's at the same time, the baseline's moved up and down at the same time and when I moved one of the PDA's to an other building the baseline was stable so I think both PDA's are working fine. Recently the UV-spectrum also showed " humpy" figure. the humps where about 3 nm apart. I don't if this problem is related tho the first one.
So, what might be wrong? people sugested that the power-suply of our lab may be the problem. Any one knows how to test this?
Somebody else sugested magnatic interferance. How do I test this?
Any other sugestens welkom.
thanks.
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By Janice Ensing on Thursday, October 14, 1999 - 01:26 pm:
My guess would be the power supply. To test, get a surge-protector to put between your current power supply and the detector and see if the problem disappears.
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By Phil on Wednesday, October 20, 1999 - 07:59 pm:
Another guess is that the PDA's are located in close proximity to air conditioning vents.
We have 2 Waters 996 PDA detectors which behave exactly as the original poster described, so badly in fact that the Waters Tech could not get the detectors to pass IQ/OQ without switching the air con off. We had conditioned power thru UPS so power supply should not have been a factor in the wavy baseline in our case.
Funnily enough, our UV-vis detectors in the same room don't show the same behaviour. Anyone know why?
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By fin on Sunday, October 24, 1999 - 04:05 am:
dear phil,
thanks for your mesage. Did you figure out was coused the problem. was it a magnatic interference or was it temperature based?
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