Analysis of asprin

Chromatography Forum: LC Archives: Analysis of asprin
Top of pagePrevious messageNext messageBottom of pageLink to this message  By bun0170414 on Tuesday, October 26, 1999 - 09:42 am:

I have found that methanol is a ineffective solvent for t.l.c analysis of asprin could any one recomend a more effective one


Top of pagePrevious messageNext messageBottom of pageLink to this message  By Anonymous on Tuesday, October 26, 1999 - 07:34 pm:

I'm assuming from the question that you're a student, so I'll get you to answer your own question.

Why was methanol ineffective?
- asprin spot moved too fast (with the "solvent front)?
- aspirin spot moved too slow (stayed at the "origin")?
- aspirin spot streaked?

Also, what type of TLC plate (silica?, bonded reversed-phase?).

More questions will follow once you answer these!


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