SPE method to quantitate hydrocodone and codeine by gcms

Chromatography Forum: LC Archives: SPE method to quantitate hydrocodone and codeine by gcms
Top of pagePrevious messageNext messageBottom of pageLink to this message  By arizona on Monday, December 6, 1999 - 06:20 pm:

I need to quantitate hydrocodone bitartrate and codeine in separate pharmaceutical syrups to discern if it meets claim. I need an SPE method or some quick way to extract to quantitate by gc/ms. Can someone recommend a sample prep procedure or decent ref.for one. I don't operate LC and the LC operator never used THF ,so that method is not being considered now. arizpaul@aol.com
617-983-6653


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